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Proton nuclear magnetic resonance ( 1 H NMR, 400 MHz, D 2 O) revealed signals at δH 2.21 (q, 2H, H-3), 2.59 (td, 2H, H-4), 2.98 (dd, 2H, CH 2 S), 3.86 (t, 1H, H-2), 4.02 (s, 2H, H-10), and 4.60 (t, 1H, H-7)